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1 article(s) from Arnold, Alexandre A.

Synthesis and solvodynamic diameter measurements of closely related mannodendrimers for the study of multivalent carbohydrate–protein interactions

Yoann M. Chabre,
Alex Papadopoulos,
Alexandre A. Arnold and
René Roy

Beilstein J. Org. Chem. 2014, 10, 1524–1535, doi:10.3762/bjoc.10.157

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Scheme 1: Synthesis of mannosylated trimers 5 and 9 using trimesic acid core transformed into propargylated (2...

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Scheme 2: Divergent CuAAc “click reaction” between propargylated core 10 and azide 3 to afford 9-mer 12.

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Scheme 3: Divergent CuAAc synthesis of “extended” 9-mer 17 using phloroglucinol (13) as core, bromoacylated T...

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Scheme 4: Convergent synthesis of further “extended” 9-mer 21 using mannosylated bromoacyl dendron 18 transfo...

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Scheme 5: Convergent assembly of 27-mer 23 using key propargylated scaffold precursors 10 and mannosylated az...

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Figure 1: a) Decay of ¹H signal for the nonavalent mannosylated compound 12 in D₂O during the PFGSTE experime...

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Published 04 Jul 2014

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